| Titre : |
Synthèse et etude structurale des complexes à base des Métaux de transition et des dérivés de la sulfanilamide |
| Type de document : |
texte imprimé |
| Auteurs : |
Sabrina Benmebarek, Auteur ; M'hamed Boudraa, Directeur de thèse |
| Editeur : |
جامعة الإخوة منتوري قسنطينة |
| Année de publication : |
2017 |
| Importance : |
182 f. |
| Format : |
30 cm. |
| Note générale : |
2 copies imprimées disponibles
|
| Langues : |
Français (fre) |
| Catégories : |
Français - Anglais
Chimie
|
| Tags : |
Sulfanilamide ligands solvent co-ligand transition metal complex X-ray
diffraction thermal decomposition Ligands sulfanilamide solvant complexe de métaux de transition diffraction RX décomposition thermique |
| Index. décimale : |
540 Chimie et sciences connexes |
| Résumé : |
Given to the ability of the derived sulfonamide to coordinate with the metal atoms in
various ways, considerable interest in synthesis and structural characterization aspects of new
complexes has appeared.
In this work, we based on the chemical ability of the sulfonamide ligand to act by these two
functions: the function -S(O)2N(H)- and the aromatic amino function -NH2 led us to
characterize the original complexes based on sulfanilamide ligand. A zinc-based mononuclear
complex and a molybdum-based polymer, characterized by X-ray diffraction, infrared
spectroscopy and TG thermogravimetric analysis, carried out by studying hydrogen bonds.
Two other polymer complexes of cobalt and copper, characterized by X-ray diffraction,
carried out by the study of hydrogen bonds. Three other organic compounds of nitro benzene
sulphynil in the ortho position have been characterized by X-ray diffraction, generates the
study of the interactions, graphs and models of the hydrogen bonds. |
| Diplôme : |
Doctorat en sciences |
| En ligne : |
../theses/chimie/BEN7094.pdf |
| Format de la ressource électronique : |
pdf |
| Permalink : |
index.php?lvl=notice_display&id=10510 |
Synthèse et etude structurale des complexes à base des Métaux de transition et des dérivés de la sulfanilamide [texte imprimé] / Sabrina Benmebarek, Auteur ; M'hamed Boudraa, Directeur de thèse . - جامعة الإخوة منتوري قسنطينة, 2017 . - 182 f. ; 30 cm. 2 copies imprimées disponibles
Langues : Français ( fre)
| Catégories : |
Français - Anglais
Chimie
|
| Tags : |
Sulfanilamide ligands solvent co-ligand transition metal complex X-ray
diffraction thermal decomposition Ligands sulfanilamide solvant complexe de métaux de transition diffraction RX décomposition thermique |
| Index. décimale : |
540 Chimie et sciences connexes |
| Résumé : |
Given to the ability of the derived sulfonamide to coordinate with the metal atoms in
various ways, considerable interest in synthesis and structural characterization aspects of new
complexes has appeared.
In this work, we based on the chemical ability of the sulfonamide ligand to act by these two
functions: the function -S(O)2N(H)- and the aromatic amino function -NH2 led us to
characterize the original complexes based on sulfanilamide ligand. A zinc-based mononuclear
complex and a molybdum-based polymer, characterized by X-ray diffraction, infrared
spectroscopy and TG thermogravimetric analysis, carried out by studying hydrogen bonds.
Two other polymer complexes of cobalt and copper, characterized by X-ray diffraction,
carried out by the study of hydrogen bonds. Three other organic compounds of nitro benzene
sulphynil in the ortho position have been characterized by X-ray diffraction, generates the
study of the interactions, graphs and models of the hydrogen bonds. |
| Diplôme : |
Doctorat en sciences |
| En ligne : |
../theses/chimie/BEN7094.pdf |
| Format de la ressource électronique : |
pdf |
| Permalink : |
index.php?lvl=notice_display&id=10510 |
|
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